BS en 1593-1999 NDT - Leak Testing - Bubble Emission

BS EN 1593:1999

BRITISH STANDARD

Incorporating Amendment No. 1

Non-destructive testing — Leak Leak te test stin ing g — Bub Bubbl ble e emission techniques

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The European Standard EN 1593:1999, with the incorporation of amendment amendment A1:2003 has the status of a British Standard Standard

ICS 19.100

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BS EN 1593:1999

National foreword ` ` ` ` , , ` ` , , , , , , , ` ` , , ` ` ` ` , , , ` ` , ` ` , , ` , , ` , ` , , ` -

This British Standard is the official English language version of EN 1593:1999, including amendment A1:2003. The UK participation in its preparation was entrusted to Technical Committee WEE/46, Non-destructive testing, which has the responsibility to: —

aid enquirers to understand the text;

—

present to the responsible international/European committee any enquiries on the interpretation, or proposals for change, and keep the UK interests informed;

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monitor related international and European developments and promulgate them in the UK.

A list of organizations represented on this committee can be obtained on request to its secretary. Cross-references The British Standards which implement international or European publications referred to in this document may be found in the BSI Catalogue under the section entitled “International Standards Correspondence Index”, or by using the “Search” facility of the BSI Electronic Catalogue or of British Standards Online. This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations.

Summary of pages This document comprises a front cover, an in side front cover, the EN title page, pages 2 to 11 and a back cover. This British Standard, having been prepared under the direction of the Engineering Sector Committee, was published under the authority of the Standards Committee and comes into effect on 15 December 1999

The BSI copyright notice displayed in this document indicates when the document was last issued.

Amendments issued since publication Amd. No. 14967

Date 1 March 2004

Comments Modification to Foreword page and deletion of Annex ZA

© BSI 1 March 2004

ISBN 0 580 35166 1

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EUROPEAN STANDARD

EN 1593

NORME EUROPÉENNE

September 1999

+ A1

EUROPÄISCHE NORM

December 2003

ICS 19.100

English version

Non-destructive testing – Leak testing – Bubble emission techniques (includes amendment A1:2003) Essais non destructifs – Contrôle d’étanchéité – Contrôle à la bulle (inclut l’amendement A!:2003)

Zerstörungsfreie Prüfung – Dichtheitsprüfung – Blasenprüfverfahren (enthält Änderung A!:2003)

This European Standard was approved by CEN on 16 August 1999, and amendment A1 was approved by CEN on 20 November 2003. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal, Slovakia, Spain, Sweden, Switzerland and United Kingdom.

EUROPEAN COMMITTEE FOR STANDARDIZATION COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG

Management Centre: rue de Stassart, 36

© 1999 CEN

B-1050 Brussels

All rights of exploitation in any form and by any means reserved worldwide for CEN national Members.

Ref. No. EN 1593:1999 + A1:2003 E

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Page 2 EN 1593:1999

Contents Page Foreword

3

1 Scope

4

2 Normative references

4

3 Definitions

4

4 Personnel qualification

4

5 Principle

4

6 General requirements

5

7 Interferences

6

8 Immersion technique

6

9 Liquid application technique

7

10 Test report

8

Annex A (informative) Example of quantitative evaluation of leakage rate



10

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Page 3 EN 1593:1999

Foreword This European Standard has been prepared by Technical Committee CEN/TC 138 "Nondestructive testing", the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by March 2000, and conflicting national standards shall be withdrawn at the latest by March 2000. This document has been prepared under a mandate given to CEN by the European Commission and the European Free Trade Association. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and the United Kingdom.

Foreword to amendment A1 This document EN 1593:1999/A1:2003 has been prepared by Technical Committee CEN/TC 138 "Non-destructive testing", the secretariat of which is held by AFNOR. This Amendment to the European Standard EN 1593:1999 shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by June 2004, and conflicting national standards shall be withdrawn at the latest by June 2004. This document has been prepared under a mandate given to CEN by the European Commission and the European Free Trade Association. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal, Slovakia, Spain, Sweden, Switzerland and the United Kingdom. ` , , ` , ` , , ` , , ` ` , ` ` , , , ` ` ` ` , , ` ` , , , , , , , ` ` , , ` ` ` ` -



Page 4 EN 1593:1999

1 Scope This European Standard describes procedures for the detection and location of leaks by the bubble emission techniques. The sensitivity depends on techniques and materials used. Two techniques are described: a) immersion technique: quantitative measurements can be made using this procedure with particular devices (see informative annex A). b) liquid application technique. This standard can be used for equipment which can be evacuated or pressurised.

2 Normative references This standard incorporates by dated or undated reference, provisions from other publications. These normative references are cited at the appropriate places in the text and the publications are listed hereafter. For dated references, subsequent amendments to or revisions of any of these publications apply to this standard only when incorporated in it by amendment or revision. For undated references the latest edition of the publication referred to applies. EN 473

Qualification and certification of NDT personnel - General principles

EN 1330-8

Non-destructive testing - Terminology - Part 8 - Terms used in leak tightness testing

EN 1779:1999

Non-destructive testing - Leak testing – Criteria for method and technique selection

3 Definitions For the purposes of this standard, the definitions given in EN 1330-8 apply.

4 Personnel qualification It is assumed that leak testing is performed by qualified and capable personnel. In order to prove this qualification, it is recommended to certify the personnel in accordance with EN 473 or equivalent.

5 Principle The techniques involve the establishment of a pressure difference across the object wall and the observation of bubble formation in a liquid medium located on the low pressure side. The minimum detectable leakage rate by these techniques depends on the pressure difference, the gas and the liquid used for testing.



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Page 5 EN 1593:1999 6 General requirements The position of the leak shall be visible directly or indirectly in order to check if it is a real leak in the area to be tested. 6.1 Gases The test gas is normally air. Inert gases may however be used. When inert gases are used, the safety aspects of oxygen deficient atmospheres shall be considered. 6.2 Pressure limits Verification shall be obtained that the object has been designed to withstand the test pressure difference. The test conditions shall be such that the object is not permanently deformed nor should the test be a hazard for the operators. 6.3 Stabilization time (for immersion technique) Prior to examination, the test pressure in the sealed object shall be maintained for a time appropriate for the establishment of bubble emission. For small leaks, this may take several minutes. 6.4 Surface temperature Normally the temperature of that part of the surface of the object that is to be examined shall o not be below 278 K (5 C) nor above 323 K (50 °C), throughout the examination. Local heating or cooling is permitted provided the temperatures remain within this range. Where it is impractical to comply with the foregoing temperature limitations, other temperatures may be used provided that the procedure has been shown to be suitable. 6.5 Direct visual examination Direct visual examination is usually made when the surface can be viewed directly at a distance not exceeding 0,6 m at an angle not less than 1/6 rad (30 degrees). Mirrors may be used to improve the angle of vision, and aids such as magnifying lenses may also be used to assist examinations. The component or area under immediate examination should be illuminated, if necessary with a flashlight or other auxiliary lighting, to attain an appropriate light level. Recommended illumination is 350 lux to 500 lux. 6.6 Indirect visual examination In some cases indirect visual examination may have to be substituted for direct examination. This may involve the use of visual aids such as mirrors, endoscopes, telescopes or other suitable instruments. These should have a resolution capability at least equivalent to that obtainable by a direct visual observation.



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Page 6 EN 1593:1999 7 Interferences The test object should be thoroughly cleaned. Surface contamination, e.g. grease, rust, weld slag, etc., on the test object surface can mask or cause bubble formation and give a false indication. Contaminated detection liquid or one that foams spontaneously on application may cause spurious surface bubbles on the test object and should be avoided.

8 Immersion technique 8.1 General This technique (see EN 1779:1999, table A.2, technique C.1) is applicable to the examination of objects that can be completely immersed in a container of detection liquid, including sealed or temporary sealed ones during the test, and the pressure in any part of the test object shall be greater than in the liquid and should be known. 8.2 Variations 8.2.1 Direct pressurization of the object The object is pressurized and placed in the selected detection liquid. The surface, after the stabilization (soak) time, is observed for a minimum period which depends on the test specification (e.g. allowable leakage rate, pressure, liquid type) and the type of test object. A stream of bubbles originating from any isolated point shall be interpreted as a leakage. 8.2.2 Use of detection liquid at elevated temperature If the object is sealed close to an atmospheric pressure, its internal pressure can be increased by placing it in the detection liquid held at an elevated temperature. The test time depends on the internal volume of the object and shall be sufficient to allow a suitable pressure increase within the object (according to the equation of state of ideal gases). The efficiency of this test can be increased by introducing, before sealing, a liquid with a boiling point lower than the test temperature. A stream of bubbles originating from any isolated point shall be interpreted as a leakage. 8.2.3 Use of vacuum The sealed object is completely immersed in the detection liquid in a vacuum chamber, with a viewing port (see figure 1). Pressure in the vacuum chamber is reduced to a level which depends on the detection liquid, to prevent excessive loss of liquid by evaporation. A series of bubbles originating from any isolated point shall be interpreted as a leakage.

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Page 7 EN 1593:1999 8.3 Detection liquids used in immersion technique Various liquids may be used for the detection, provided that they are transparent enough and do not adversely affect the objects being tested. Commonly-used are water with suitable wetting agents, ethylene glycol or low-viscosity mineral oil. An analysis of the detection fluid should be carried out to determine the presence of undesirable components, such chlorine, fluorine, sulfur, etc. Mineral oil is the most suitable liquid for the vacuum technique, but degreasing of the test object may be necessary. When the vacuum technique is used the liquid should be previously degassed.

9 Liquid application technique 9.1 General This technique involves the application of a liquid film to the surface of the test object. It is applicable to any object in which a pressure differential can be created across the boundary to be examined. This technique may be used for open components and for those objects for which immersion would be impractical. 9.2 Variations 9.2.1 Direct pressurization of the object This procedure (see EN 1779:1999, table A.2, technique C.2) refers to objects that can be pressurized. A suitable liquid surfactant is applied on the low pressure side (by brush, spray or other methods). Afterwards, wait for a sufficiently long inspection time to realise even slow production of foam from small leaks. From large leaks the test fluid may be blown away and no foaming may occur. A growing foam originating from any isolated point shall be interpreted as a leakage. 9.2.2 Use of vacuum for unpressurized (open) objects This technique (See EN 1779:1999, table A.2, technique C.3) is suitable for open objects e.g. unfinished parts, objects not accessible on the rear side or large objects for which the pressurization is impractical. The method involves the attachment of a suitable vacuum box with a top viewing port to those parts of the test object under investigation, the latter having been previously covered with surfactant liquid (see figure 2). Care shall be taken in the design and construction of the vacuum box to prevent implosion.



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Page 8 EN 1593:1999 The required pressure can be attained in the box by any convenient method, e.g. a vacuum pump. Care should be taken in the sealing of the vacuum box, particularly on the weld reinforcement (crown). The pressure should be progressively reduced until the specified test pressure, e.g. 20 kPa or 50 kPa, has been reached. This value has to be maintained for the specified time, at least 30 s. A minimum vacuum box overlap of 50 mm for adjacent test areas is necessary. 9.3 Detection liquids used in liquid application technique Suitable surfactant liquids shall be used. They shall be nonvolatile (they shall not dry at test temperature during the inspection time), viscous and shall not foam under reduced pressure. Commercial fluids not specific for leak testing shall not be used unless their suitability has been previously demonstrated on that type of test, by comparison with the characters of a specific bubble test fluid. In the presence of gas leakage however the bubbles which form should persist for the duration of the test. For vertical surface tests, the test fluid viscosity may be increased, if necessary, by suitable methods. The compatibility of the test fluids with the materials of the test objects has to be ensured.

10 Test report If procedures require a test report, this shall include the following information: ` ` ` ` , , ` ` , , , , , , , ` ` , , ` ` ` ` , , , ` ` , ` ` , , ` , , ` , ` , , ` -

a) technique used; b) internal and/or low side pressure; c) liquid type; d) test temperature; e) soaking time; f) duration of the test; g) operator certification; h) test results.



N R C o e o p r p r y e r p o i d g r u o h d c t e u B c d r t i i b t o i n y s h H S o I r S t n a e u n n d t w d a o e r d r k r l s i i n c I g e n n s p s t i e e t u r m t

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w i

i t i o t n t e h d B w S i I t h o U u n t c l i o c n e t n r s o l l e e d f r o C m o p I H y S

N L i o c t e f n o r s R e e e = s F a u l l o e , r 1 C 2 o / 2 r 0 p / 2 n 0 o 0 4 F 2 P 0 P : P 4 5 V : 1 p 1 e r M a S d T m i n i s t r a t o r / u s e n e w u / 2 1 1 0 5 0 3 1 0 6 , U s e r = L a p w

1 vacuum gauge 2 to vacuum pump 3 detection liquid 4 bubble formation 5 object 6 viewing port

1 2 3 4 5 6 7

test section of the object with detection liquid viewing port vacuum gauge to vacuum pump vacuum box object soft rubber seal

Figure 1: Immersion technique with use of vacuum

Figure 2: Use of liquid application technique for unpressurized (open) objects

Page 10 EN 1593:1999

Annex A (informative) Example of quantitative evaluation of leakage rate The bubble test is generally specified for the location of leaks and in this context the leakage rate is not required as any bubble formation means rejection. In some cases, e.g. a valve with a metallic gasket, the maximum specified leakage may be accepted. In this case the leakage can be evaluated by bubble counting or can be measured by accumulating the escaping gas in a graduated tube. A typical test arrangement for the determination of the leakage rate is shown in figure A.1. The gas escaping from the object (i.e. a safety relief valve) is led through a small tube to bubble in a transparent cup or collected and accumulated in a graduated tube. Before starting the bubble count, the test pressure shall be applied for a period in a range depending on the object size. Air at approximately ambient temperature should be used. Using table A.1, the leakage rate can be estimated from the size and number of bubbles per unit time. Table A.1

Page 10 EN 1593:1999

Annex A (informative) Example of quantitative evaluation of leakage rate The bubble test is generally specified for the location of leaks and in this context the leakage rate is not required as any bubble formation means rejection. In some cases, e.g. a valve with a metallic gasket, the maximum specified leakage may be accepted. In this case the leakage can be evaluated by bubble counting or can be measured by accumulating the escaping gas in a graduated tube. A typical test arrangement for the determination of the leakage rate is shown in figure A.1. The gas escaping from the object (i.e. a safety relief valve) is led through a small tube to bubble in a transparent cup or collected and accumulated in a graduated tube. Before starting the bubble count, the test pressure shall be applied for a period in a range depending on the object size. Air at approximately ambient temperature should be used. Using table A.1, the leakage rate can be estimated from the size and number of bubbles per unit time. Table A.1

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Page 11 EN 1593:1999

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1 seal 2 cover plate 3 pressure NOTE: The cover plate should be fitted with a suitable device to relieve body pressure in case of accidental popping of the valve seal.

Figure A.1 Test apparatus for valve seat leak testing



BS EN 1593:1999

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BS en 1593-1999 NDT - Leak Testing - Bubble Emission

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